A laboratory scale spray dryer
An instruction manual
The first point
A technical parameters
Inlet air temperature control: 0-300 C
Outlet temperature control: 0-120 C
Evaporation of water: 2000ml/H
The maximum feed rate: 2000 ml/H
Electric heater power: 2.5KW AC220V single phase +
Fan: 0.2KW maximum air volume 5.5 m fand /min maximum wind pressure686Pa
Compressed air working pressure: 2-5Bar
Air compressor: 0.25KW the maximum production of 4.2 m fand /h measure
Size: 780*620*1600 (mm) L*W*H equipment
Nozzle caliber; 0.75mm
Weight: 170KG
Two scope of application
The machine is mainly suitable for Laboratory of liquid materials directly intomicro powder, without before drying of material in filtration, concentration andgrinding, for all solutions such as emulsion, suspending liquid with broad-spectrum applicability.
Three、The random component
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Serial number
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Parts name
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Number
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1
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Small laboratory spray drier
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1
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2
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The exhaust pipe 4 meters
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1
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3
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A feeding tube 10 meters
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1
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4
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Pipe 2 meters
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1
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5
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Glass device
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Glass drying chamber
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3
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Glass tube
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3
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Glass bottle
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4
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Cyclone separator
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3
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6
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The nozzle size 0.75mm
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1
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7
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A magnetic stirrer device
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1
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Original manufacturers factory, wooden packaging, high temperature machine, high pressure identification
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Four installation instructions
A) drying chamber is provided with both hands and then inserted into the drying room drying room stall fixed splint (on white PTFE pad), five for lockinghandle.
B) cyclone separator installation will cyclone separator the tightening nut, a sealing ring and a stainless steel gasket is sheathed in the cyclone air outlet pipe, and the air outlet pipe is inserted into the device together, regulating the drying chamber and an air outlet of the cyclone separator inlet position, thetwo mouth straight alignment, with clamp connection two mouth, finally the tightening nut tightening of cyclone separator.
C) will aggregate bottle and a cyclone separator are connected by screw thread connector
D) will set the feeding tube and the drying chamber are connected by screw thread connector
E spray chamber) will be installed on the device, connect the 4mm tracheal(needle used) and 6mm (spray) blue trachea
F food grade silicone tube) mounted to a peristaltic pump, and inserted into the spray chamber inlet
Note: all glassware for fragile handle with care, pay attention to installation andcleaning
Make sure all the components have been installed in place and then power onoperation
The operation five
Peristaltic pump: click on the "open", a peristaltic pump "start", then click "stop the closure. The automatic control of peristaltic pump running, click theautomatic button blue zone peristaltic pump (below) (buttons into a" closed "),automatically start the peristaltic pump, according to the set valueautomatically adjust the rotary speed of the peristaltic pump air temperature,feed rate and the peristaltic pump, then click on the manual operation,automatic display"".
Control of fan fan start and stop button, click on the fan zone (above), the blower is started (move to the "start" button, click below), the blower stops(button to move to "stop").
The needle through needle start and stop control, click through button blackzone (above), by starting (move to the "start" button, click below), by stopping(button to move to the "stop"), needle running speed in the interface (three)by changing the needle setting value set to change the running speed.
Control of air compressor air compressor start and stop button, click on the air compressor black zone (above), air compressor (move to the "start" button,click below), the air compressor stops (button to move to "stop").
Heater for starting control of electric heater and heater button click stop, blackarea (above), the heater starts (move to "start" button, click below), the heater stops (button to move to "stop").
Note: the heater before fan didn't start is not start, turn off the fan heaterautomatically disconnect.
Fan set rotation frequency setting machine, press the numerical box, pop-upnumeric keyboard, digital reset by pressing the CLR key, and then enter the desired value, press the ENTER key to modify the finished.
Peristaltic pump manual control peristaltic pump operation, automatic buttonblack area click peristaltic pump (above) (ON), automatic start, peristaltic pump shown below, a peristaltic pump stop (OFF)
Needle set by running frequency needle, a numerical representation of a few seconds to start again, press the numerical box, pop-up numeric keyboard,digital reset by pressing the CLR key, and then enter the desired value, press the ENTER key to modify the finished.
Peristaltic pump set of feed quantity r/m set of peristaltic pump), press thenumerical box, pop-up numeric keyboard, digital reset by pressing the CLR key, and then enter the desired value, press the ENTER key to modify the finished.
Instructions: click control panel to enter the interface (two), to enter theinterface click on the main menu (a)
Inlet air temperature self stability regulating inlet air temperature, when and only when dry found inlet air temperature display value and the inlet airtemperature setting value between the fluctuations are larger, the need forinlet air temperature self regulating, to ensure that the inlet air temperaturesetting value and the inlet air temperature display value consistent, open self adjustment before must ensure that the inlet air temperature setting value and the inlet air temperature display 50 degrees above the temperature value,such as the inlet air temperature setting value at 120 degrees, the temperature of inlet wind shown in the below 70 degrees, i.e. the set value >display value above 50 degrees.
Click the inlet air temperature self adjusting button black zone (above) (ON),inlet air temperature self regulating start. Require completed automatically end, as in the self regulating unfinished referred to in the preceding paragraph shall end self regulating, click the inlet air temperature self adjustable end button.
Note: the fan and the heater after the start of inlet air temperature self regulating function,
Inlet air temperature setpoint of inlet air temperature, press the numerical box,pop-up numeric keyboard, digital reset by pressing the CLR key, and then enter the desired value, press the ENTER key to modify the finished.
Inlet air temperature display values show the actual value of the inlet air temperature
Inlet air temperature self adjustable end block in the process of self adjustment of inlet air temperature, want to interrupt self regulating, press this button
Outlet air temperature self regulating when and only when the drying room and find out the wind temperature display value and the air outlet temperature setting value between the relatively large fluctuations, the need for air temperature self regulating, to ensure that the outlet temperature setting value and temperature of air in the displayed value consistent, open note moneymust ensure that the outlet temperature setting value and the outlet air temperature showed a temperature difference between the values of theabove 50 degrees, such as air temperature set at 70 degrees, outlet air temperature display values at or above 120 degrees, namely the displayed value > set the value to 50 degrees.
Outlet air temperature setpoint outlet air temperature, press the numericalbox, pop-up numeric keyboard, digital reset by pressing the CLR key, and then enter the desired value, press the ENTER key to modify the finished.
Outlet air temperature display values show the actual air temperature value
Outlet air temperature self adjustable end when in the process of outlet air temperature self regulating of want to interrupt, self regulating, press this button
Excluding the six common problems
The problem may be the reason and solve method
1 fan does not work, the intermediate relay R201.2 damage damage to the drive fan is damaged, replace the R201.2
2, the electric heater does not work, the fan does not start SSR201 solid state relay to damage electric heater is broken, the blower is started to replace theSSR201 solid state relay
3, air compressor does not work, the intermediate relay R201.1 damaged air compressor start air compressor damaged, replace the R201.1 start air compressor
4, no electrical equipment, plus the socket is not reliable circuit breaker NFB in the closed position, check the external power source whether electric open NFB
5, HMI touch screen no display panel work, start button switch power supplydamage damage damage intermediate relay R1.2 touch screen is damaged,replace the start button to replace the switching power supply to replace the R1.2
6, the PLC does not work, NFB circuit breaker in the closed positionintermediate relay R1.1 damage of PLC damage, open NFB to replace the R1.1
7, the temperature of inlet wind no display, PT-100 temperature probe is connected to loose PT-100 damage to the PT temperature module damage,fastening
8, out of the wind temperature no display, PT-100 temperature probe is connected to loose PT-100 damage to the PT temperature module damage,fastening
9, inlet air temperature can not reach the set value, the fan air volume is too large, modify the parameters of fan
10, the air inlet temperature fluctuations, the PID value is not accurate, forinlet air temperature self regulating
The 11 air outlet temperature can not reach the set value, the air flow into thetoo big (peristaltic pump manual), modify the peristaltic pump parameters
12 out of the wind temperature fluctuations, the PID value is not accurate, forair temperature self regulating
13 drying chamber bottom dropping material, inlet air temperature is too lowatomization air pressure too low compressed air feed quantity is too big,increase the temperature of inlet wind device open rear cover plate will adjust the pressure to 2-3Bar (phi 6 Blue trachea) check whether everywhere connection leak modify peristaltic pump parameters
14 needle does not work, the valve is not open air pressure is too small to set too high electromagnetic valve damage needle parameters, open the valve(phi 4 white trachea) adjustable high pressure relief valve pressuremodification through needle parameters for electromagnetic valve
Seven, experiment preparation
1 follow the installation instructions, each component will be installed
2 press the device blue start button, start the blower, the heater is started
The 3 set of inlet air temperature and air temperature value
4 stay out of the wind temperature reaches the set value, the peristaltic pumpautomatically open
5 advanced water, observe the changes of temperature atomization andmaterial, from the new set of fan, inlet air temperature, or air outlet temperature, stay stable rear feeding
Eight, stop steps
1 when the material is used up, will all the material in the water inlet hose after spray (about 5 minutes), close the peristaltic pump
2 close the air compressor
3 turn off the heater
4 until the inlet air temperature dropped to 90 degrees below, shut down the wind machine
5 remove the aggregate bottle, transfer the material to the other container
The 6 container after cooling completely remove the cleaning
Name of Institution: Shanghai Jipad Instrument Co.,Ltd
Address: Shanghai Minhang District Pujiang Caohejing Development Zone
Tel: 021-61722009
Mobile phone: 18721606967
Jipad-2000ML實驗室噴霧干燥機
產(chǎn)品說明:
Jipad-2000ML實驗室噴霧干燥機主要適用于高校、研究所和食品醫(yī)藥化工企業(yè)實驗室生產(chǎn)微量顆粒粉末，對所有溶液如乳濁液、懸浮液具有廣譜適用性,適用于對熱敏感性物的干燥如生物制品、生物農(nóng)藥、酶制劑等，因所噴出的物料只是在噴成霧狀大小顆粒時才受到高溫，故只是瞬間受熱，能保持這些活性材料在干燥后仍維持其活性成份不受破壞。
Jipad-2000ML實驗室噴霧干燥機
產(chǎn)品特征：
1、采用彩色大觸摸屏操作，全自動控制和手動控制相結合，國內(nèi)*：
2、全自動控制：一鍵式開機，設定噴霧工藝參數(shù)后，溫度到達預定溫度，蠕動泵自行啟動，觸摸屏上顯示運行動畫，運行流程清晰顯示；關機時只需按停止鍵，機器自動**關機。
3、手動控制：如需在實驗過程對工藝參數(shù)進行調(diào)整，可方便切換至手動狀態(tài)，整個實驗過程彩色觸摸屏動態(tài)顯示（動畫）。
4、關機保護功能：關機時只需按停止鍵，機器除風機外立即停止運行，保證設備不會因為誤操作（強行關風機）而導致加熱部分燒壞。
5、噴霧、烘干及收集系統(tǒng)采用透明的上等高硼硅耐熱玻璃材料制造，使得噴霧干燥過程在無污染及穩(wěn)定的環(huán)境下進行，且使整個噴霧干燥實驗進程可直接觀察，為科研人員掌控實驗進程及實驗結果提供了極大的便利,并能及時發(fā)現(xiàn)解決問題。所有玻璃元件易拆卸，易清洗。
6、內(nèi)置進口全無油空壓機，噴粉的顆徑呈正態(tài)分布，流動性非常好，而且噪音非常低，小于60db，符合國家實驗室噪音標準；
7、二流體噴霧的霧化結構，整機采用上等不銹鋼材料精密制造，設計緊湊，無需附屬設備，方便使用，歷久如新。
8、為了滿足用戶在實驗范圍調(diào)節(jié)各項參數(shù)的要求，在干燥溫度控制的設計上采用實時調(diào)控PID恒溫控制技術，使全溫區(qū)控溫準確，加熱控溫精度±1℃。
9、為了保持樣品的純凈，配備了進風口過濾器。
10、進料量可通過進料蠕動泵調(diào)節(jié)，小樣品量可達50ml。磁力攪拌器可選
11、干燥后的成品干粉，其顆粒度較均勻，95%以上的干粉在同一顆粒度范圍。
12、小型噴霧干燥機針對黏性物料，設有噴咀清潔器（通針），在噴咀被堵塞時，會自動**，通針的頻率可自動調(diào)整；
13、**的塔壁吹掃裝置，物料回收率更高。
Jipad-2000ML實驗室噴霧干燥機
技術參數(shù):
1、噴霧干燥機全自動控制與手動控制雙重控制模式，整個實驗過程彩色觸摸屏動態(tài)顯示（動畫）
2、進風溫度控制：30℃～300℃
3、出風溫度控制：30℃～140℃
4、蒸發(fā)水量：1500mL/H～2000ml/h
5、大進料量：蠕動泵可調(diào)大為2000ml/h
6、小進料量：50mL
7、可升級成雙級分離收集系統(tǒng)
8、實時調(diào)控PID恒溫控制技術，加熱控溫精度：±1℃
9、干燥時間：1.0～1.5S
10、具有關機保護功能：關機時只需按停止鍵，機器除風機外立即停止運行，保證設備不會因為誤操作（強行關風機）而導致加熱部分燒壞。
11、彩色LCD觸摸屏參數(shù)顯示：進風口溫度/出風口溫度/蠕動泵轉速/風量/通針頻率
12、噴嘴口徑：0.5mm/0.7mm/0.75mm/1.0mm/1.5mm/2.0mm可選，并可根據(jù)要求定制
13、設有噴咀清潔器（通針），在噴咀被堵塞時，會自動**，通針的頻率可自動調(diào)整
14、噴霧干燥機整機全不銹鋼制作,二流體噴霧的霧化結構，噴霧、烘干及收集系統(tǒng)采用透明的上等高硼硅耐熱玻璃材料制造
15、內(nèi)置進口全無油空壓機，噴粉的顆徑呈正態(tài)分布，流動性好，而且噪音非常低，符合國家實驗室噪音標準；
16、整機功率：3KW/220V
17、塔壁吹掃裝置，物料得率更高
18、噴霧頭冷卻裝置（可選）
19、可直接升級成應用于有機溶劑物料干燥的氮氣循環(huán)系統(tǒng)
20、設備尺寸：1200mm(高）×650mm（長）×500mm（寬）
上海旌派儀器有限公司
公司電話：021-61722009 公司傳真：021-34790213
網(wǎng)址：http://shjipad.goepe.com/
上海旌派儀器有限公司(Shanghai Jipad Instrument Co.,Ltd);坐落于上海市浦江鎮(zhèn)***園區(qū)漕河涇開發(fā)區(qū)，是一家從事恒溫設備、樣品前處理、實驗常規(guī)配套設備開發(fā)設計、制造、經(jīng)營 銷售的**技術企業(yè)，被評為上海市級優(yōu)良企業(yè)。擁有產(chǎn)品研發(fā)團隊和一支技能有素、實踐經(jīng)驗豐富的**技師組成的生產(chǎn)團隊，為能制造出性能優(yōu)良、質量可靠的產(chǎn)品奠定了堅實的基礎。
上海旌派儀器有限公司(原上海恒溫設備廠)是規(guī)模較大的科學儀器制造商，我公司主要生產(chǎn)無菌均質器、氮吹儀、高低溫恒溫槽、雪花制冰機、三用恒溫水箱、恒溫水浴鍋、超聲波細胞粉碎 機、超聲波清洗機、超凈工作臺、生物**柜、脂肪測定儀等，產(chǎn)品覆蓋樣品處理、破碎、恒溫等各個領域，并成功打造國內(nèi)**自主品牌Jipad。旌派產(chǎn)品在研發(fā)、生產(chǎn)、調(diào)試、檢驗、試驗 等每一個生產(chǎn)環(huán)節(jié)都嚴格貫徹ISO9001：2000質量體系指令。公司產(chǎn)品廣泛的服務于化工、石油、國防、物理、化學、生物工程、醫(yī)藥衛(wèi)生、生命科學、環(huán)境工程、高等院校、科研機構等領域 ，多年來，覆蓋了國內(nèi)近三十個省市、自治區(qū)。
我們崇尚"誠信、專業(yè)、服務"的企業(yè)理念；樹立"做**企業(yè)、創(chuàng)知名品牌"的發(fā)展目標；貫徹"以市場為導向、以技術為基礎、以服務為根本"的經(jīng)營理念；實現(xiàn)"讓用戶滿意"的服務宗旨；履 行"****合格出品精益求精周到服務"的承諾。
上海旌派全體員工歡迎各位同行、各位合作之友、各位用戶與我們攜手共同致力于國家科研儀器的發(fā)展，共同追求屬于我們的未來。上海旌派承諾：凡從我公司購買的產(chǎn)品一律三包一年，提 供終身售后服務。
